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KMID : 1059520120560010078
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Journal of the Korean Chemical Society
2012 Volume.56 No. 1 p.78 ~ p.81
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New Synthesis of Perhydrotriazolotriazoles Catalyzed by TiCl4 under Ambient Conditions
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Safari J.
Gandomi Ravandi S.
Ghotbinejad M.
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Abstract
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Aromatic 2,3-diazabuta-1,3-dienes in glacial acetic acid with isothiocyanate in the presence of catalyst TiCl4 at room temperature produced via criss-cross cycloaddition reactions the corresponding perhydro[1,2,4]triazolo[1,2-a][1,2,4] triazole-1,5-dithiones in relatively high yields and short reaction time.
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KEYWORD
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Criss cross cycloaddition, Azine, Catalyst, Perhydrotriazolotriazole
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